Advanced Analytical Chemistry 310-ERS-CAZE
Wykład (WYK) Rok akademicki 2024/25

Literature available from the person conducting the course.

The following learning outcomes will be achieved as a result of the course: KP7_WG1, KP7_WG2. Verification of the achievement of the learning outcomes will be based on the result of the written exam.

The prerequisite for admission to the exam is a passing grade in the laboratory. Final exam in written form.

The importance of analytical chemistry, the role of analytical tools. The analytical process and the characteristics of its various stages. Basic concepts related to it: sample, signal, measurement principle (analytical technique), analytical method, analytical procedure. Analytical composition, distribution, structural, process analytics. The concept of trace analysis and its specifics. Errors of chemical analysis and the causes of their formation. Principles and methods of sampling. Sampling of solid materials, samplers for solid sampling. Techniques for reducing the solid sample. Sampling of bulk, chunk, soil, plant materials, bottom sediments. Collection of gaseous and liquid samples. Methods of storing and transporting solid, liquid and gaseous samples. Documentation of the sampling stage, control of the sample preparation process. Typical operations of the sample preparation stage for analysis. Methods of dissolution of inorganic and organic samples. Methods of separation and concentration of analytes, elimination of interfering substances and matrix effects. Calibration of analytical methods. Validation of analytical methods - parameters of the validation process. Recent developments and directions in analytical chemistry: green analytical chemistry; miniaturization in sample preparation for analysis; miniature chemical sensors; flow and coupled techniques; multifunctional molecular materials in chemical analysis; porous, magnetic and nanomaterials; speciation and speciation analysis.

Lecture with elements of student activation